To lower the temperature, you need to decrease the temperature by decreasing the pressure. CannaCommunity is a forum-based community that is broken up to every aspect of your life that you'd want to know about. Forging a New Genetic Frontier in Cannabis. Not vacuumed
I have not tried it but intend to. Do not blindly follow advice found here. -Pyrex dish 8x8, amazon ($16ea) Posted Image Simply put a small amount of ISO or everclear in your dish prior to blasting, just enough to coat the bottom of the dish you are using for small runs and more if you are making ounces. Parchment Paper and even the oil slick pads will deposit microscopic silicone particles into your extraction.
-Electric hot pans for float dishes and the griddle for the vacuum oven, amazon ($40ea) http://forum.grassci...ax-shatter.html It specifically states that the transfer of Cannabis from one state to another is completely prohibited. Still not done.
I use two float dishes and separate the first two from the third. PLEASE READ: All information on this web site was provided by members and guests who have freely given their ideas. Water bath: 120f-130f until reaction stops. Water bath: 100f until it starts to puff up, then agitate it some with a fork to pop the bubbles.
Put on you safety glasses and Extract the cans through the cylinder all at once into the pyrex dish while its floating in the water. THE GUIDE: Vacuum oven: Vacuum at -29inhg and 160f until no reaction. Now that you have extracted you BHO and you have the right equipment, it’s time to get to the vacuum purging.
Chose the temprature you want to use and start extracting. Posted Image However, I cannot control every post; thus, one must read the following posts with HESITANCE since I do not recommend reading any information and believing its the TRUTH! Never blast onto anything other than pyrex. It causes the Silicone to swell and flake off into your extraction. 3. At this temperature, the butane is past its dissolving point and … Leave it for 30 minutes, depressurise, and then back to 29” HG. My cylinders are glass, 1.5" diameter, and 10 through 14 inches long. These use alcohol and are known as polar secondary extractions, or winterization. Pre-Vacuum Purging. Water bath: 100f-150f until reaction stops.
The poor mans vacuum oven. Purge times and temps: Keep it thin or it will still trapalcohol.
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How about this Also when using a griddle to warm a vacuum chamber or water bath realize the surface temp of the griddle is going to be higher than inside the chamber.
So I dont think the speed in which you degas is important beyond not damaging your extract with a direct blast of air. To remove the solvent from the mixture, you need to "purge it" in a vacuum oven. Posted Image Just make sure you extend your purge times a significant amount to allow the alcohol to evaporate all the way off. -Honey is the purest and most activated and is achieved at temps up to 190. The third is the clearest and the first two will knock you flat. Before using ANY information, ideas, or methods of growing, using, selling, or refining Cannabis that you learn here; you must consult your doctor or a qualified licensed medical provider to make sure they are…. Allow to purge in the float dishes until reaction slows or stops. Posted Image Posted Image make sure it is floating freely. -Oven Allow to heat to 100f-110f, allow to sit in the oven for about 30 min. -Vacuum pump 1.5 cfm ac vac pump goes to -29inhg/14psi from amazon($90) I recommend a 2 stage but they cost more. Temperature: All the temps are taken with a inferred thermometer and are surface temps. These temps are different for everyone but they are close and are consistent for the vacuum purge method. Posted Image
4. Once desired temp is reached let it sit until there is no reaction and surface is like glass. This can take 24-48 hours. BHO blasted into ISO Oven: 160f-180f until no reaction. Only the cold wax/erl and honeys seem to keep for extended times. The temp does not really matter as long as it is not to hot. Posted Image Do this several times over a ten min period. Also it is best to mark your dial on the griddle where certain temps are. They can also be used to clean up your product by removing any lipids, waxes, fats and other non polar compounds you may not want in your product. To … Posted Image -Vacuum chamber round polystyrene($90) or converted pressure canning pot. Posted Image
This is the step that makes it so clear and not black or green. -Point and shoot inferred thermometer The temperature you use from start to finish will determine the finishing state. To vacuum the solvents out of your BHO, you will need at least three items: Vacuum Compressor; Vacuum Chamber; Vacuum Connector Pipe; The first step is to take the BHO and place it on something like a silicone pad that typically comes with most extraction kits.
Heat lowers the viscosity, so I heat the material in a thin film until it reaches that state, but no hotter. -Hard wax is slightly activated and is achieved at temps up to 140.
Set the griddle at the desired temp using the thermometer to check your extraction at regular intervals to ensure it does not over heat. Set up the electric skillet and float the pyrex dish in it in water. This allows the BHO to remain liquid and for the butane to more easily escape without getting trapped. 2 ounces after a vacuum. Place the shatter inside the vacuum oven and set the temperature to 90 degrees Fahrenheit. 2. The lower the temp the longer it will need to be purged. Posted Image
OUTSIDE WITH FIRE EXTINGUISHERS READY!!!! How to purge BHO without a vacuum setup.
This is the original thread and has some good info throughout. Just make sure you extend your purge times a significant amount to … I degas my chamber in as little as 5 seconds. This is why you dehydrate. Remember you want to run the dehydrator at a lower temp than you plan to finish with. This allows the BHO to remain liquid and for the butane to more easily escape without getting trapped. -Budder/hash/honey comb is not something I usually make as they are not stable and degrade fast. 6. Do this outside. Like the color?
These forums are moderated for accuracy, any misguidance, internet trolls, and legality compliance. Then vacuum to 29inhg for no more than 30 min at this temperature. Purge times and temps: Dont allow them to dry out, empty immediately when they are still iced over. Posted Image Where ever you fall on the Cannabis Spectrum, we have the information you need! This is the final step of making shatter. Now this looks really nice but what happens under -29inhg? Why we vacuum In that regard I feel that honey is the best to store long term as it is the most concentrated and purged of the lot, but a properly made shatter or wax will also keep. Posted Image However, this may take a longer duration.
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